Using a calibrated leak standard allows these to be measured and subtracted from the overall reading. American society for testing and materials, standard practice for leaks using the mass spectrometer leak detector in the detector probe mode, astm e499e499m11, west conshohocken, pa, 2011. Helium massspectrometer leakdetector calibration scitation avs. Standard practice for leaks using the mass spectrometer. In the past, the leak detection companies had been used different gases in tracer gas leak detection method, e. However, steam turbines are challenging environments for leak detection due to high temperatures and the fact that the test media is water vapor, which can. Data system mass detector analyzer vacuum system source inlet region more precisely mass spectrometry determines the mass of a molecule. The helium mass spectrometer leak detection system is used to identify both large gross and small leaks in a product. Helium leak detection testing elabs has multiple varian, mass spectrometer helium leak detectors for finding leaks as small as 1x1010 ccsec. Introduction to helium mass spectrometer leak detection varian associates on.
Vs series helium operation manual mass spectrometer. How to perform a leak check with a helium mass spectrometer. Principle of helium leak detector the mass spectrometer leak detector is a complete system for localization and measuring of leaks inside or outside of a product. However, in the helium mass spectrometer leak detection method, the sensitivity, or resolution, of the instrument is often the only component of. Currently, the helium leak test, a deterministic method, is being established as the gold standard for its sensitivity and versatility. International journal of engineering research and general. Varians helium leak detection technologies a mass spectrometer leak detector msld is a complete system for locating andor measuring the size of leaks into or out of a device or a container. This is done using a commercial test leak, which generates a known and reproducible test gas rate under defined conditions. Agilent varian vs mr15 mobile helium mass spectrometer leak detector with ds 302, ds302 rotary vane vacuum pump, 120v, g8601a, varian mr15 leak detector, vsmr15 helium leak detector, agilent leak detector, vsmr15 leak detector, leak detector service.
Helium mass spectrometry based upon astm f 239105 1 is applicable to nonporous packaging such as vials, syringes and cartridges. Mass spectrometer leak test performed at eb industries. Agilent varian vs mr15 mobile helium mass spectrometer. The agilent vs helium leak detector combines the simplicity of twobutton operation with advanced expert system intelligence. They are sensitive to system outgassing and a number of background effects. This varian 956 portatest ii mass spectrometer leak detector is used and in excellent condition. The system pressurizes a product with dry air and then completes a gross leak check to determine if a large leak exists. Helium mass spectrometer leak detector radio spectrum. It is important to specify an acceptable leak rate for each vacuum system. Introduction to helium mass spectrometer leak detection. Traditionally, nasa used four massspectrometer based leak detection systems for each launch support. A highresolution quadrupole mass spectrometer hrqms that we have recently developed. The instruments sensitivity and efficiency are ideal.
Helium mass spectrometer leak detection high quality vacuum. Helium is relatively expensive when compared to other industrial gases, so wasting it in the case of a big leak is very costly. These units are used both purely as residual gas analyzers or process gas analyzers as well as for leak detection. This method of leak detection is initiated when a tracer gas, helium, is introduced to a test part that is connected to the msld system. Agilent varian vs mr15 mobile helium mass spectrometer leak. Good for leak detection as large as 1 std ccsec and up to 10 11 std ccsec. A helium leakage test is performed with the help of a helium leak detector known as a mass spectrometer leak detector msld. The operating principle of quadrupole mass spectrometers is shown in chapter 6. Furthermore, helium leak detection offers the capability also to locate the position of a leak. Information regarding the various leak detection methods is given in appendix a introduction to leak detection. Extremely sensitive and reliable quantitative measurement capability makes it very important for systems and components which require exact leak rate specification.
Operation manual mass vs series helium leak detectors. Using the spectron 5000 to leak check heat exchangers. It is important to remember that background concentration in. Heliot is a universal modern leak detector designed to implement all methods of mass spectrometry leak test in accordance with european standarts. Portable helium leak detector provides accurate registration of the flow of helium up to 1. The most sensitive and safe device, however, is a mass spectrometer with 180 magnetic sector field optimized for the detection of mass 4. Tracer gas leak detection with helium gas water leak. Standard practice for leaks using the mass spectrometer leak. The test may be conducted on any device or component across which a pressure differential of helium or other suitable tracer gas may be created, and on which the effluent side of the leak to be tested is accessible for probing with the mass spectrometer sampling probe. Models 959 and 959d operations manual mass spectrometer. Lacos suite of titantest helium mass spectrometer leak detectors bring you powerful solutions targeting the unique challenges of todays leak testing applications.
A helium massspectrometer is the instrument best suited for detecting it i. At the origin of the helium leak detection method was the manhattan project and. Helium leak detection mass spectrometer is used for helium leak detection method. Standard helium conditions are always present during helium leak detection for a vacuum system when the system is connected to a leak detector.
Feb 17, 2014 helium mass spectrometer leak detection is preferred for detecting and mitigating leaks in steambased power generation systems. Dec 18, 2019 a helium leakage test is performed with the help of a helium leak detector known as a mass spectrometer leak detector msld. They generally do not like knocks, shocks or being switched on and off repeatedly. Vs series helium mass spectrometer leak detectors agilent. Varian vacuum products, introduction to helium mass spectrometer leak detection, second edition, 1995. A helium mass spectrometer is the instrument best suited for detecting it i. There are many more leak detection methods but none of them is as accurate localization and quantification as helium leak detection method. Our leak detectors feature automated startup and calibration for maximum productivity, built in application setups, and an array of accessories to make any leak detection process simple. The machine checks for gross leaks using a pressure decay method during which helium mass spectrometer leak test system read more. Helium leakage tests are performed on pipelines, storage tankages and vessels that store chemicals, crude oil, petroleum products or other liquid materials to detect small leaks in these sealed industrial containers. Model 959 and 959d mass spectrometer helium leak detectors.
We typically use it to perform leak detection of our cryostats and associated equipment that will be flowing hydrogen at cryogenic temperatures, often through a high vacuum environment. New agilent technologies vs md30 mobile helium mass. We are capable of leak testing to pressures up 20,000 psi using nitrogen and 80 read more. A lowcost alternative to helium is forming gas, typically a mixture of 5% hydrogen and 95% nitrogen that can be used as a safe, nonflammable, and effective tracer gas in many applications.
A mass spectrometer gas analyzer can be used in tracer gas leak testing to detect helium or hydrogen escaping from a microleak. Virtually every part we manufacture that goes into a vacuum or critical atmospheres is leak tested on an industry standard helium mass spectrometer leak detector. By convention, m is the numerical value for the mass of the ion and z is the numerical value for the charge of the ion. Vactron company represents heliot helium mass spectrometer leak detector and provides services and maintenance training. A circular hole with a diameter d 1 cm in the wall of. Jul 30, 2014 when it comes to finding leaks in your furnace, it can be a true art form. Helium mass spectrometer leak detectors are used in production line industries such as refrigeration and air conditioning, automotive parts, carbonated beverage containers food packages and aerosol packaging, as well as in the manufacture of steam products, gas bottles, fire extinguishers, tire valves, and numerous other products including all. The helium mass spectrometer, although much more robust these days, is really a laboratory piece of equipment that can be used in production. The helium mass spectrometer based leak testing has been widely used in the industry for fine leak detection 8,9. The basic functions of leak detection are the detection, location and size measurement of leaks in sealed systems. Mass spectroscopy leak sensors employ helium as the gas target 5, 6.
The pcu helium mass spectrometer leak test system is a compact easy to operate ultra fine leak test system. Mass spectrometer leak detector how is mass spectrometer leak detector abbreviated. The mass to charge ratio mz is used to describe ions observed in mass spectrometry. Tracer gas leak test systems leak detection equipment. Meet the demands of your leak testing process with a featurerich design and an unparalleled choice of options and accessories. Mass spectroscopy applied to gas leak detection and fuel ionization by. Helium leak testing is the most sensitive of the common leak testing methods, and covers a wide range of methods that utilize a helium mass spectrometer leak detector such as lacos titantest helium leak detector. High vacuum technology has been finding uses in increased number of industrial applications. This ranges from robot helium sniffing to high speed helium leak testing and to high vacuum helium leak testing the helium mass spectrometer, although much more robust these days, is really a laboratory piece of equipment that can be used in production. Agilent varian 956 portatest ii mass spectrometer leak detector.
Mass spectrometer leak detector how is mass spectrometer. Agilent vs md30 mobile helium mass spectrometer leak detector with triscroll 620 dry scroll vacuum pump, 120v, vsmd301, g8601b, md30 leak detector, agilent vs30 leak detector, agilent helium leak detector, agilent leak detector. The helium leak detector is a portable, highly sensitive instrument designed to detect helium carrier gas leaks in thermal desorption and gc systems. This system embodies pcus field proven testing technology in combination with modern electronic control, compact industrial design and simplified operator use. Standard methods of test for leaks using the mass spectrometer leak detector astm e 49373,1916 race st. Volume 47, issues 68, juneaugust 1996, pages 767769. Helium leak tests were performed at room temperature 22 0c. Vacusolv can also be used for fine cleaning of other parts in the leak detectors vacuum system, such as valves and fittings.
Fundamentals of leak detection in order to achieve an overview of the correlation between the geometric size of the hole and the associated leak rate it is possible to operate on the basis of the following, rough estimate. Measurements of true leak rates of mems packages mdpi. Advancements in helium leak detection for disk drive. A mass spectrometer gas analyzer can be used in tracer gas leak testing to detect helium or hydrogen escaping from a micro leak. Tqc has considerable experience in integrating mass spectrometers into production systems for leak testing various parts. Leak detection with other boc edwards instruments in applications where the highest sensitivity of the mass spectrometer leak detector is not required, or where the application demands the detection. This standard prescribes procedures to be used for calibrating leak detectors of the mass spectrometer type. The leak detecting method by helium mass spectrometer has advantages of high sensitivity, high speed and extensive range of application, comparing with methods of bubble recognition, pressure attenuation and halogen leak detection, etc. Helium leak detector is most widely used method in the industries. This unit is complete and functional however the cover for left side function keys is missing.
Especially so, in the case of development of nuclear components which calls for a high degree of vacuum tightness and a reliable leak detection method which can detect minutest leak paths. Hhv s mass spectrometer leak detector is a complete system used for locating and measuring the size of the leak either into or out of a device or a container. Vs series helium mass spectrometer leak detectors d r a f t 1 2 1 3 1 0 warranty products manufactured by seller are warranted against defects in materials and workmanship for twelve 12 months from date of shipment thereof to customer, and sellers liability under valid war. It was initially developed in the manhattan project during world war ii to find extremely small leaks in the gas diffusion process of uranium enrichment plants. Many times, parts are tested more than once during the production process.
If the system is pumped down too p less than 1 mbar and if it is sprayed with helium mass 4, one refers to the spray technique. Helium leak tests were performed using a varian 979 helium leak tester, which uses a mass spectrometer to determine the leak rate, with mass flow sensitivity of 1010 s. Helium leak detector and its different applications along with various leak detection methods are described. Gas leaks are indicated with both an indicator lamp display and an audible alarm. Helium mass spectrometer leak detector hmsld fundamentals learned in bvp, it provides an introduction to production testing of parts against leakrate. Whereas leak detector has an easy to use interface, it is technically complex product. The leak detector must be calibrated in order to determine leakage rates. The mass spectrometer is used to detect the leak with helium gas. One of ipsens most common customer questions concerns how to find a leak using a helium mass spectrometer. Request pdf leak detection, calibrations and reference flows. A helium mass spectrometer is an instrument commonly used to detect and locate small leaks. It is important to remember that background concentration in air is a limiting factor for any tracer gas detector. Helium mass spectrometer leak detector mass spectrometer leak detector is used for locating and measuring the size of the leak. When it comes to finding leaks in your furnace, it can be a true art form.
Products manufactured by seller are warranted against defects in materials and workmanship for twelve 12 months from date of shipment thereof to customer, and sellers liability under valid war. Helium mass spectrometer leak detection high quality. A highresolution quadrupole mass spectrometer hrqms that we have recently developed, can detect a 4he population as small as 104 peak in a dz atmosphere. Thus, the hrqms has been applied to detect he leaks. Laco provides leak standards for a number of major helium mass spectrometer brands including lacos titantest leak detector. Sensitive helium leak detection in a deuterium atmosphere. A circular hole with a diameter d 1 cm in the wall of a vacuum vessel is closed with a valve.
Helium is the best choice to find leaks because it is nontoxic, inert, noncondensable, nonflammable, present in the atmosphere in trace amounts 5 ppm. The detection of these cracks involves the use of a light tracer gas which is capable. Using a ls70 helium detector to find underground plumbing leaks 2885 country dr. Mass spectrometer leak detector serves to test the leaktightness of various systems and facilities which allow pumping the inner cavity or objects filled with helium or a gas mixture containing helium, and the detection and localisation of leakage sites leaks. Step 1 characterization of the helium mass spectrometer leak detector the first step is to characterize the helium msld with respect to the four measurement uncertainty components of resolution, repeatability, hysteresis, and drift. This ranges from robot helium sniffing to high speed helium leak testing and to high vacuum helium leak testing. Due to its small atomic size, helium passes easily through leaks. Model 979 series helium mass spectrometer leak detector draft 91503 iii warranty products manufactured by seller are warranted against defects in materials and workmanship for. This paper gives an introduction about leak detection of vacuum system. Using an optimized mass spectrometer and helium as tracer gas, leak rates down to.
The agilent vs helium leak detector combines the simplicity of two. Sep 09, 2010 mass spectrometer leak test performed at eb industries. Leak detection is used to detect microopenings, porosities, etc. Vs series leak detectors from agilents vacuum products division use a mass spectrometer and high vacuum pump to provide a much higher level of sensitivity and accuracy than sensorbased helium leak detectors. In applications where leak rates of components or systems are evaluated against a leak rate requirement, the uncertainty of the measured leak rate must be included in the reported result. One part of he in 200,000 parts of air can be detected.
Apr 15, 2004 a simple low resolution mass spectrometer is described which has been used successfully in detecting small leaks in high vacuum equipment. This paper will give an introduction to the leak detection of vacuum. Using a ls70 helium detector to find underground plumbing. But today, most of the companies preferred to use helium gas to detect a leak because of its superior sensitivity. These methods can be implemented in simple, manuallyoperated benchtop systems or in highly automated high volume production systems.